This Small Molecule Crystallography Starter Kit 1 provides all essential components for mounting and collecting X-ray data from small molecules at both room and cryogenic temperatures. Designed as a comprehensive solution, it equips researchers with reliable tools for efficient crystallography workflows. Each kit contains 20 Dual Thickness MicroMounts with assorted apertures (5 each of 75, 100, 150, and 200 µm), ideal for diverse sample sizes. It also includes 1 tube of Apiezon N Cryogenic vacuum grease, crucial for maintaining cryo conditions. For sample handling and mounting, a pair of heavy-duty tweezers is provided, alongside 10 reusable goniometer bases and 10 magnetic CryoVials, ensuring secure sample attachment and storage. A detailed instruction manual guides users through the process. This kit is an indispensable resource for optimizing small molecule crystallography experiments, promoting precise data collection and reliable results.